Keywords of our Technology Microwave Reaction

1. Reduction of reaction time and yield improvement by rapid heating

2. Being capable to make an optional synthesis by reducing secondary reactions

3. Reactions that do not occur by the ordinary heating methods may occur in case of a microwave experiment.

Equipment in our possession: (We will extend our support services for scaling up the production.): μReactor Dimensions: Main Unit: 430W x 470D x 470H Controller: 320W x 265D x 150H Batch Tank-Type Reactor: Dimensions: 2100W x 710D x 1280H · Microwave frequency: 2.45GHz · Microwave Output: 40〜770W (variable) · Microwave Fixed Output Control/Automatic Temperature Control · Microwave Mode: Multi mode · Stirrer: Electromagnetic stirrer built-in · Inside Temperature accurately controlled by an optical fiber thermometer · Reaction Capacity: 10mL〜200mL · Microwave Frequency: 2.45GHz · Microwave Output: 4.5kW (1.5kW x 3) · Microwave Control: Programmed PID Control (Continuous output control,Pulse control) · Reaction Vessel: 6.5l

No. Heating Method Solvents Temperature Microwave Output Time Yield 1 Oil bath DME/H2O reflux - 15min 51.2% 2 Microwave DME/H2O reflux 70〜350W 15min 78.9%*

*The object compound was obtained with better yield, than in the case by the ordinary heating.

Keywords of our Technology

Synthesis of Functional Materials Purification by Sublimation Metal nano-sized fine powders Organic Solar Cells Pentacene Organic EL materials Dendrimer Radiation Dose Indicator Optical Active Materials Microwave Reaction Homogenous Transition Metal Catalysts